| نویسندگان | Hossienifard M., Hashemi L., Amani V., Kalateh K., Morsali A. |
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| نشریه | Journal of Inorganic and Organometallic Polymers and Materials |
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| كد DOI/DOR | 10.1007/s10904-011-9473-y |
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| تاریخ انتشار | ۲۰۱۱ |
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چکیده مقاله
A new nano-sized Zn(II) complex, [Zn(5,5′-dtbu-2,2′-bipy)Cl 2] n (1) was synthesized and its structure determined by X-ray crystallography. The new nano-sized complex was prepared at oleic acid as a surfactant at 280 °C and characterized by scanning electron microscopy, elemental analyses and IR spectroscopy. The ZnO nano-particles were synthesized from thermolysis of nano-compound 1 at 600 °C and similar compound, [Zn(5,5′-dimethyl-2,2′-bipy)Cl 2] n (2), at two different methods. SEM images show the average size of ZnO nano-particles are 78 and 50 nm for the compounds 1 and 2, respectively. © 2011 Springer Science+Business Media, LLC.
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